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Síntese e Actividades Biológicas de Triazóis-Pirazóis em Clubes

Síntese e Actividades Biológicas de Triazóis-Pirazóis em Clubes

          
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About the Book

Neste livro, foram desenvolvidos novos métodos para a síntese de 1,2,4-triazóis com pirazóis numa única estrutura molecular. Na primeira parte do estudo, as chalconas dos 3,5-difenil-1,2,4-triazóis foram investigadas como novas vias para a síntese dos compostos alvo. Depois disso, a hidrazida do ácido isonicotínico foi reagida com as chalconas em meio ligeiramente ácido para obter os compostos alvo em rendimentos bons a excelentes. Subsequentemente, as mesmas reacções foram realizadas com hidrato de hidrazina, que forneceu os pirazóis correspondentes em bons rendimentos. As estruturas de todos os pirazóis substituídos foram confirmadas por IR, 1H-NMR, espetroscopia de massa e análise elementar. Todas as reacções foram monitorizadas por TLC. Na segunda parte do estudo, os derivados finais foram analisados quanto à sua atividade antinociceptiva e antimicrobiana. A atividade antinociceptiva foi realizada através de métodos analgésicos centrais e periféricos. O estudo da propriedade antimicrobiana foi realizado através do método do caldo líquido. Todos os compostos apresentaram atividade analgésica a uma dose de 100 mg/kg. Todos os pirazóis substituídos exibiram uma poderosa atividade antimicrobiana numa gama de MIC de 62,50- 15,62 µg/ml.


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Product Details
  • ISBN-13: 9786207345281
  • Publisher: KS Omniscriptum Publishing
  • Publisher Imprint: Our Knowledge Publishing
  • Height: 229 mm
  • No of Pages: 76
  • Spine Width: 5 mm
  • Width: 152 mm
  • ISBN-10: 6207345282
  • Publisher Date: 02 Apr 2024
  • Binding: Paperback
  • Language: Portuguese
  • Returnable: N
  • Weight: 122 gr


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