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Systematische Untersuchungen Der Tetrachloridoaluminate Und -Gallate Von Schweren Elementen Der Gruppe 14

Systematische Untersuchungen Der Tetrachloridoaluminate Und -Gallate Von Schweren Elementen Der Gruppe 14

          
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About the Book

Im Bereich der modernen Festkorperchemie ist die Charakterisierung neuer Strukturen seit jeher von grossem Interesse. Diesbezuglich konnten bis heute im Bereich der Phasenchemie der ternaren Hauptgruppenmetallhalogenide eine Vielzahl an Verbindungen strukturchemisch aufgeklart werden. Jedoch sind kaum Ergebnisse zur intermediaren Verbindungsbildung in den Systemen SnCl_2-AlCl_3bzw. PbCl_2-AlCl_3literaturbekannt. So konnte im Zuge dieser Arbeit das Phasendiagramm des Systems PbCl_2-AlCl_3mittels thermoanalytischen Messungen und temperaturabhangigen Rontgenpulveraufnahmen erstellt werden. Weiterhin ist es gelungen intermediare Verbindungen in den oben genannten Systemen mittels Rontgenbeugung am Einkristall bzw. mittels Rietveld-Verfeinerung am polykristallinen Pulver strukturchemisch zu charakterisieren. Zudem konnte die intermediare Verbindungsbildung in den Phasensystemen SnCl_2-GaCl_3bzw. PbCl_2-GaCl_3erfolgreich untersucht und strukturelle Gemeinsamkeiten zu den jeweiligen Tetrachloridoaluminaten belegt werden. Letztlich gelang es, drei intermediare Verbindungen des bis dato nicht untersuchten Systems GeCl_2-AlCl_3durch Komproportionierungsreaktion von Germanium mit Germanium(IV)-chlorid in Anwesenheit von Aluminiumchlorid herzustellen und strukturchemisch zu charakterisieren. Erstmalig lassen sich damit verlassliche Parameter fur die Ge^II-Cl-Bindungsbeziehung zur Abschatzung der Bindungssituation des Ge(II)-Kations mit Hilfe des bond-valence-Konzepts ableiten.


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Product Details
  • ISBN-13: 9783832542931
  • Publisher: Logos Verlag Berlin
  • Binding: Paperback
  • No of Pages: 159
  • Series Title: German
  • ISBN-10: 3832542930
  • Publisher Date: 10 Jul 2016
  • Language: German
  • Returnable: N
  • Weight: 448 gr

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