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Synthese Und Anwendung Planar-Chiraler [2.2]paracyclophanliganden Mit N-Donorfunktionen Und Deren Ubergangsmetallkomplexe Zur Synthese Substituierter Amine

Synthese Und Anwendung Planar-Chiraler [2.2]paracyclophanliganden Mit N-Donorfunktionen Und Deren Ubergangsmetallkomplexe Zur Synthese Substituierter Amine

          
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About the Book

Seit der Entdeckung des [2.2]Paracyclophans durch Brown und Farthing 1949 wurden diese besonderen Kohlenwasserstoffe vielfach erfolgreich fur Anwendungen in der asymmetrischen Synthese eingesetzt. Dennoch erschweren bis heute die strukturellen und elektronischen Eigenschaften des [2.2]Paracyclophan-Grundgerusts seine synthetische Einsetzbarkeit als planar-chirales Analogon eines Phenylrings. Im ersten Teil dieser Arbeit wurde daher eine Syntheseroute zu verschiedenen mono- und disubstituierten [2.2]Paracyclophanen mit zusatzlichen Stickstoffheterocyclen erarbeitet, die bei Metallkoordination stabile funfgliedrige Metallacyclen ausbilden konnen. Dabei wird durch die Etablierung eines Stille-Kreuzkupplungsprotokolls eine modulare Synthese von isomeren mono- und disubstituierten Pyridyl[2.2]paracyclophanen vorgestellt. Daruber hinaus wird die Darstellung kationischer Rutheniumkomplexe uber eine diastereoselektive Cycloruthenierung unter C-H-Aktivierung des [2.2]Paracyclophangerusts besprochen. Neben Ruthenium-komplexen konnten auch Kupfer(I)-komplexe gemischter P, N-Liganden synthetisiert werden, wobei uberraschenderweise eine Phosphinierung einer Stille-Kupplung bevorzugt wird. Im zweiten Teil der Arbeit konnte die Eignung [2.2]Paracyclophan-basierter N, O-Chelatliganden fur die Hydroaminierung und Hydroaminoalkylierung demonstriert werden. Dazu wurden zunachst Syntheserouten zu den racemischen und enantiomerenreinen Liganden entwickelt, bevor deren Titan- und Tantalkomplexe in der Hydroaminierung und Hydroaminoalkylierung eingesetzt wurden.


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Product Details
  • ISBN-13: 9783832545291
  • Publisher: Logos Verlag
  • Publisher Imprint: Logos Verlag Berlin
  • Height: 210 mm
  • No of Pages: 348
  • Series Title: Beitrage Zur Organischen Synthese
  • Weight: 700 gr
  • ISBN-10: 3832545298
  • Publisher Date: 31 Jul 2017
  • Binding: Paperback
  • Language: German
  • Returnable: N
  • Spine Width: 0 mm
  • Width: 145 mm


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