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Sintesis de Zeolita TS-1 con porosidad jerarquizada para su aplicacion en epoxidacion de olefinas

Sintesis de Zeolita TS-1 con porosidad jerarquizada para su aplicacion en epoxidacion de olefinas

          
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About the Book

Tesis Doctoral / Disertación del año 2009 en eltema Biología - Otros temas, Nota: 10.0, Idioma: Español, Resumen: En el presente trabajo, se plantea la obtención de zeolita TS1 con porosidad jerarquizada mediante un proceso basado en la silanización de núcleos zeolíticos. Dicho método, ha sido aplicado previamente en la síntesis de materiales zeolíticos tipo ZSM5, ZSM11 y Al Beta con porosidad jerarquizada, obteniendo excelentes resultados en reacciones de catálisis ácida. No obstante, dicho método no ha sido utilizado aún en la síntesis de materiales zeolíticos con propiedades redox, entre los que destaca la zeolita TS1. La síntesis de este tipo de materiales permitiría reducir las restricciones estéricas y difusionales derivadas del pequeño tamaño los microporos zeolíticos, posibilitando su aplicación en reacciones que involucren moléculas voluminosas, como son los hidroperóxidos orgánicos. La utilización de este tipo de oxidantes adquiere especial relevancia cuando se desean llevar a cabo reacciones en medios libres de agua, en los que la presencia de ésta pueda afectar a la distribución de productos. Es por ello que el principal objetivo de la presente Tesis Doctoral es la síntesis y caracterización de materiales zeolíticos tipo TS1 con porosidad jerarquizada mediante el método basado en la silanización de núcleos zeolíticos, para posteriormente estudiar su actividad catalítica en reacciones de epoxidación de olefinas utilizando peróxido de hidrógeno e hidroperóxidos orgánicos como agentes de oxidación. De acuerdo con lo anteriormente expuesto, el plan de investigación propuesto se ha realizado a través de las siguientes etapas: Síntesis de zeolita TS1 con porosidad jerarquizada a partir de xerogeles SiO2 TiO2 impregnados con TPAOH. Con objeto de optimizar el procedimiento de preparación planteado, se estudiaron como variables de síntesis: el tipo de agente silanizante, el tiempo de precristalización, la relación másica TPAOH/xerogel empleada durante la etapa


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Product Details
  • ISBN-13: 9783656217978
  • Publisher: Grin Publishing
  • Binding: Paperback
  • Language: Spanish
  • Returnable: N
  • Spine Width: 19 mm
  • Width: 148 mm
  • ISBN-10: 3656217971
  • Publisher Date: 19 Jun 2012
  • Height: 210 mm
  • No of Pages: 330
  • Series Title: Spanish
  • Weight: 430 gr


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